N,N-diethylaniline was synthesized under normal tempreture with tetraethyl ammonium hydroxide as phase transfer catalyst.
以苯胺和溴烷为原料,用四
基氢氧
铵作相转移催
,在常压下
N,N
基苯胺。
N,N-diethylaniline was synthesized under normal tempreture with tetraethyl ammonium hydroxide as phase transfer catalyst.
以苯胺和溴烷为原料,用四
基氢氧
铵作相转移催
,在常压下
N,N
基苯胺。
The content of ethoxyl group in obtained product was 43.98%.
该法所得基纤维素产品的
氧基含量为43.98%。
N,N-diethylaniline was synthesized from aniline with bromoethane using tetraethylammonium chloride as phase transfer catalyst under atmospheric presure.
用四基氯
胺作相转移催
可在常压下由苯胺和溴
烷
N,N-
基苯胺。
The solvent effect on the synthesis of diethylaluminum azide(DEAA) from diethylaluminum chloride(DECA) and sodium azide(NaN3) is discussed.
以氯基铝(DECA)和叠氮
钠为原料
基叠氮铝(DEAA)时,反应介质的溶
性质不同,产物及其收率也不同。
Catalytic synthesis of phenetole by ethylation of phenol with diethyl carbonate(DEC)in fixed bed reactor was investigated.
以碳酯(DEC)为
基
试
,与苯酚在气固相条件下催
苯
醚。
Synthesis of ethyl iso nicotinate using BTEAC (benzyl triethyl ammonium chloride) as phase transfer catalyst was studied.
以BTEAC(苄基三基氯
铵)为相转移催
了异烟
酯。
The major components were Triphenylmethane, Phytol, n-Hexadecanoic acid, Phenol, 2,4,6-tris (1,1-dimethylethyl).And etc.
其主要分是三苯基-甲烷、叶绿醇、正十六碳
、2,4,6-三(1,1-
甲
基)-苯酚等,这为进一步开发利用蒌蒿提供了科学依据。
Activated carbon as the sorbent and catalyst support was capsulated with ethyl cellulose by phase separation methods.
摘要对兼具吸附和催载体功能的多孔结构活性炭,以
基纤维素为材料用相分离进行包覆。
Objective:To study the preventive effect of Matrine(MT) and Oxymatrime(OMT)on rat hepatoma induced by diethylnitrosamine(DEN).
研究苦参碱(MT)和氧苦参碱(OMT)分别对
基亚硝胺(DEN)诱发大鼠肝癌的预防阻断作用。
Tetraethyl thiuram disulfide was synthesized one step from diethylamine and carbon bisulfide with hydrogen peroxide(27.5%) as oxidant.
以胺和
硫
碳为原料,经双氧水(275%)氧
,一步
了四
基秋兰姆
硫。
The p-fluorophenoxy propionic acid was synthesized by p-fluorophenol and 3-chloropropanoic acid as row materials and transfer catalyzed by TEBA.
以对氟苯酚和3-氯丙为起始原料,用苄基三
基氯
铵作为催
,经过相转移催
对氟苯氧丙
。
By means of cyanoethylation and chlorination,wood sawdust was converted into thermoplastic material and then compounded with short sisal fibers.
通过氰基
反应,使木粉转
为热塑性材料,再与短切剑麻纤维混
,热压制得植物纤维增强塑
植物纤维基复
材料。
Two kinds of bis-hydroxyalkyl or bis-methyl formylate subtituted bis-ethylenedithio-tetrathiafulvalenes (BEDT-TTF) and their charger-transfer complexes (CT-complexes ) with TCNQ were synthesized.
了带双羟烷基及双甲
甲酯基取代的两种双
硫代亚
基四硫代富瓦烯(BEDT-TTF)的衍生物及其它们与TCNQ的CT-络
物。
Trimethylaluminum(TMA),usually used in organic catalysis and organic synthesis,was synthesized by reaction of triethylaluminium (TEA) with methyl bromide on iron-stibonium complex catalyst.
用新的催体系(铁-锑复
催
)催
三
基铝(TEA)与溴甲烷进行烷基交换反应
三甲基铝(TMA)。
The mixture was refined by sodium sulfide and sodium hydroxide to afford an O,O-diethyl thiophosphoryl chloride at a purity of 99%.
该粗品通过精制工艺的改进,采用硫钠和氢氧
钠的混
物进行处理,得到纯度≥99%的O,O-
基硫代磷酰氯。
Ethyl cellulose was synthesized successfully in one step based on reaction of cellulose with excess chloroethane and sodium hydroxide in toluene as diluent.
采用纤维素与过量的氯烷及氢氧
钠反应,以甲苯为稀释
,用一步法
功地
了
基纤维素。
Etodolac was synthesized with 7-ethyltryptophol and methyl 3-oxopentanoate as the starting materials.Highly pure etodolac was obtained by purifying the crude product with a mixing solvent.
以7-基色醇和3-氧代戊
甲酯为起始原料,以甲醇为溶
,
了依托度
.采用混
溶
对粗品进行精制,得到了高纯度的依托度
.
The paper studied the preparation of bromine from basic Magnesium bromide in the production of maltol and ethyl maltol, the synthesis of bromethyl from bromine, sulfur and alcothol.
研究了以麦芽酚、基麦芽酚生产中的碱式溴
镁废渣为原料制取溴;以溴、硫和
醇
溴
烷的方法。
This paper studied the new synthetic technology of taurin (2- aminoethanesulforic acid).It was synthe sized by the reaction of monoethanol amine sulfate with sodium sulfrous in yield of 85%.
研究了牛磺(2-氨
基磺
)
的新工艺:用氨基
醇硫
酯与亚硫
钠溶液反应制备,收率达85%。
Dimethyl phenylethyl carbinyl acetate (DPCA ) was synthesized by using a new catalyst. This technology decreases the pollution and can also be used in synthesis of other carbinyl acetates perfume.
用一种新型催甲基苯
基原酯(DPCA),并简
了
工艺,减少了生产过程中产生的三废,因而投入生产已具备了必要条件。这种新型催
可用于其它原酯类香料的
。
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