The mass spectra of ureide-type noncyclic polyethers with 2(3H)-benzoxazolone as end groups were studies.

研究了以2（3H）-苯并唑酮为端基、具有酰脲结构的非环多醚化合物的质谱。

The triphenylamine azo compounds were successfully characterized by matrix-assisted laser desorption-ionization time of flight mass spectrometry(MALDI-TOF MS).

利基质辅助激光解吸电离飞行时间质谱法分析三苯胺偶氮化合物。

Objective:To develop a GC-MS approach for the determination of tripropyltin(TPrT),tributyltin(TBT) and triphenyltin(TPhT) in fish.

建立水产品中三丙基锡、三丁基锡和三苯基锡的气相色谱-质谱(GC-MS)分析方法。

The deleterious ingredients in gas emission of sculpturing organic glass were studied,using gas chromatography-mass spectrometry coupled with 3-step preconcentrator.

研究了3阶段预浓缩气相色谱-质谱法检有玻璃在雕刻过程中排放的有害气体的组成。

Besides, laser optoacoustic spectroscopy technique and laser mass spectrometry will play more important role in research of internal combustion engine.

另，激光光声光谱技术、激光质谱仪等有望在内燃的研究中发挥更大的作。

Dodecanol abietate succinic anhydride was synthesized from abietic acid.The structures of products were characterized by spectrum of IR，HNMR and MS.

以枞酸为起点，合成了十二醇酯琥珀酸酐，采光谱、核磁共振波谱及质谱对中间产物及终产物进行了结构表证。

In this paper ten lactonic crown ethers weresynthesized, of which seven were new compounds.Theirstructures were confirmed by EA,IR,1HNMR andMS analysis.

合成了10个内酯型冠醚化合物，其中7个冠醚是新化合物，其结构均由元素分析，及、核磁、质谱分析证实。

The controls were homeochronous inpatients with affective disorder and normal individuals.lsoprene breath levels were measured by gas chromatography combined with mass spectroscopy(GC-MS).

气相色谱一质谱联仪检其呼出气体中异戊二烯的浓度。

Desorption chemical ionization mass spectrometry of twelve metallohematoporphyrin complexes has been investigated under DEP condition using mixture of tetramethylsilane and methane as regent gas.

本文以四甲基硅烷／甲烷混合反应气，采DEP技术，定12个金属血卟啉络合物的解吸化学电离质谱。

Based on these results and the ESI-MS data, the mechanism of sulfoxidation was proposed to be intramolecular nucleophilic oxygen transfer to a coordinated sulfide.

基于这些结果和电喷雾质谱(ESI-MS)数据，亚砜化反应的理推为分子内亲核氧转移到络合的硫醚底物上。

The oils were analyzed by GC-MS and percentages were obtained by normalized peak areas, where main components are nootkatone, D-limonene, osthole, cis-linaloloxide, furfural, and trans.

气相色谱-质谱(GC-MS)联技术分析,鉴定出主要成分为圆柚酮、D-柠檬烯、王草素、顺式-芳樟醇氧化物、糠醛、反式-芳樟醇氧化物。

RESULTS The chlortetracycline's epimer, tetracycline and its epimer, as impurities in chlortetracycline have been determined by the liquid chromatogram and its first order mass spectrum.

结果得到金霉素样品液相色谱图以及液相色谱峰对应的一级质谱图。对谱图进行分析归纳,推金霉素样品中含有四环素、差向异构四环素和差向异构金霉素杂质组分。

Uranium isotope abundance ratio has been measured by total sample evaporation and signal integration,and a thermal surface ionization mass sepctrometry equipped with multicollector has been used.

采全蒸发技术、离子流强度积分的方式,多接收器热表面电离质谱计量铀同位素丰度。

The content of free acetic acid in cigarette smoke condensates was determined by GC-MS with isopropyl alcohol as the solvent and nonanol as the internal standard.

以异丙醇为溶剂,壬醇为内标,采气相色谱-质谱法分析了卷烟烟气总粒相物中的游离乙酸,乙酸定结果的相对标准偏差小于1%,平均回收率为99。

In this review,we described the recent development of mass spectrometry techniques for the study of peptidase structure and function in the central nerve system of Aplysia and other mollusks.

本文以海兔等软体动物为素材,综述近年来采质谱和高效液相色谱技术研究中枢神经系统多肽酶结构与功能的进展。

The mass spectra of ureide-type noncyclic polyethers with 2(3H)-benzoxazolone as end groups were studies.

研究了以2（3H）-苯并唑酮为端基、具有酰脲结构的非环多醚化合物的质谱。

The triphenylamine azo compounds were successfully characterized by matrix-assisted laser desorption-ionization time of flight mass spectrometry(MALDI-TOF MS).

利用基质辅助激光解吸电离飞行时间质谱法分三苯胺偶氮化合物。

Objective:To develop a GC-MS approach for the determination of tripropyltin(TPrT),tributyltin(TBT) and triphenyltin(TPhT) in fish.

建立水品中三丙基锡、三丁基锡和三苯基锡的气相色谱-质谱(GC-MS)分法。

The deleterious ingredients in gas emission of sculpturing organic glass were studied,using gas chromatography-mass spectrometry coupled with 3-step preconcentrator.

研究了3阶段预浓缩气相色谱-质谱法检测有机玻璃在雕刻过程中排放的有害气体的组成。

Besides, laser optoacoustic spectroscopy technique and laser mass spectrometry will play more important role in research of internal combustion engine.

另外，激光光声光谱技术、激光质谱仪等有望在内燃机的研究中发挥更大的作用。

Dodecanol abietate succinic anhydride was synthesized from abietic acid.The structures of products were characterized by spectrum of IR，HNMR and MS.

以枞酸为起点，合成了十二醇酯琥珀酸酐，采用红外光谱、核磁共振波谱质谱对中间物物进行了结构表证。

In this paper ten lactonic crown ethers weresynthesized, of which seven were new compounds.Theirstructures were confirmed by EA,IR,1HNMR andMS analysis.

合成了10个内酯型冠醚化合物，其中7个冠醚是新化合物，其结构均由元素分，红外、核磁、质谱分证实。

The controls were homeochronous inpatients with affective disorder and normal individuals.lsoprene breath levels were measured by gas chromatography combined with mass spectroscopy(GC-MS).

用气相色谱一质谱联用仪检测其呼出气体中异戊二烯的浓度。

Desorption chemical ionization mass spectrometry of twelve metallohematoporphyrin complexes has been investigated under DEP condition using mixture of tetramethylsilane and methane as regent gas.

本文以四甲基硅烷／甲烷混合反应气，采用DEP技术，测定12个金属血卟啉络合物的解吸化学电离质谱。

Based on these results and the ESI-MS data, the mechanism of sulfoxidation was proposed to be intramolecular nucleophilic oxygen transfer to a coordinated sulfide.

基于这些结果和电喷雾质谱(ESI-MS)数据，亚砜化反应的机理推测为分子内亲核氧转移到络合的硫醚底物上。

The oils were analyzed by GC-MS and percentages were obtained by normalized peak areas, where main components are nootkatone, D-limonene, osthole, cis-linaloloxide, furfural, and trans.

用气相色谱-质谱(GC-MS)联用技术分,鉴定出主要成分为圆柚酮、D-柠檬烯、王草素、顺式-芳樟醇氧化物、糠醛、反式-芳樟醇氧化物。

RESULTS The chlortetracycline's epimer, tetracycline and its epimer, as impurities in chlortetracycline have been determined by the liquid chromatogram and its first order mass spectrum.

结果得到金霉素样品液相色谱图以液相色谱峰对应的一级质谱图。对谱图进行分归纳,推测金霉素样品中含有四环素、差向异构四环素和差向异构金霉素杂质组分。

Uranium isotope abundance ratio has been measured by total sample evaporation and signal integration,and a thermal surface ionization mass sepctrometry equipped with multicollector has been used.

采用全蒸发技术、离子流强度积分的式,用多接收器热表面电离质谱计测量铀同位素丰度。

The content of free acetic acid in cigarette smoke condensates was determined by GC-MS with isopropyl alcohol as the solvent and nonanol as the internal standard.

以异丙醇为溶剂,壬醇为内标,采用气相色谱-质谱法分了卷烟烟气总粒相物中的游离乙酸,乙酸测定结果的相对标准偏差小于1%,平均回收率为99。

In this review,we described the recent development of mass spectrometry techniques for the study of peptidase structure and function in the central nerve system of Aplysia and other mollusks.

本文以海兔等软体动物为素材,综述近年来采用质谱和高效液相色谱技术研究中枢神经系统多肽酶结构与功能的进展。

The mass spectra of ureide-type noncyclic polyethers with 2(3H)-benzoxazolone as end groups were studies.

研究了以2（3H）-苯并唑酮为端、具有酰脲结构的非环多醚化合物的。

The triphenylamine azo compounds were successfully characterized by matrix-assisted laser desorption-ionization time of flight mass spectrometry(MALDI-TOF MS).

利辅助激光解吸电离飞行时间法分析三苯胺偶氮化合物。

Objective:To develop a GC-MS approach for the determination of tripropyltin(TPrT),tributyltin(TBT) and triphenyltin(TPhT) in fish.

建立水产品中三丙锡、三丁锡和三苯锡的气-(GC-MS)分析方法。

The deleterious ingredients in gas emission of sculpturing organic glass were studied,using gas chromatography-mass spectrometry coupled with 3-step preconcentrator.

研究了3阶段预浓缩气-法检测有机玻璃在雕刻过程中排放的有害气体的组成。

Besides, laser optoacoustic spectroscopy technique and laser mass spectrometry will play more important role in research of internal combustion engine.

另外，激光光声光技术、激光仪等有望在内燃机的研究中发挥更大的作。

Dodecanol abietate succinic anhydride was synthesized from abietic acid.The structures of products were characterized by spectrum of IR，HNMR and MS.

以枞酸为起点，合成了十二醇酯琥珀酸酐，采红外光、核磁共振波及对中间产物及终产物进行了结构表证。

In this paper ten lactonic crown ethers weresynthesized, of which seven were new compounds.Theirstructures were confirmed by EA,IR,1HNMR andMS analysis.

合成了10个内酯型冠醚化合物，其中7个冠醚是新化合物，其结构均由元素分析，及红外、核磁、分析证实。

The controls were homeochronous inpatients with affective disorder and normal individuals.lsoprene breath levels were measured by gas chromatography combined with mass spectroscopy(GC-MS).

气一联仪检测其呼出气体中异戊二烯的浓度。

Desorption chemical ionization mass spectrometry of twelve metallohematoporphyrin complexes has been investigated under DEP condition using mixture of tetramethylsilane and methane as regent gas.

本文以四甲硅烷／甲烷混合反应气，采DEP技术，测定12个金属血卟啉络合物的解吸化学电离。

Based on these results and the ESI-MS data, the mechanism of sulfoxidation was proposed to be intramolecular nucleophilic oxygen transfer to a coordinated sulfide.

于这些结果和电喷雾(ESI-MS)数据，亚砜化反应的机理推测为分子内亲核氧转移到络合的硫醚底物上。

The oils were analyzed by GC-MS and percentages were obtained by normalized peak areas, where main components are nootkatone, D-limonene, osthole, cis-linaloloxide, furfural, and trans.

气-(GC-MS)联技术分析,鉴定出主要成分为圆柚酮、D-柠檬烯、王草素、顺式-芳樟醇氧化物、糠醛、反式-芳樟醇氧化物。

RESULTS The chlortetracycline's epimer, tetracycline and its epimer, as impurities in chlortetracycline have been determined by the liquid chromatogram and its first order mass spectrum.

结果得到金霉素样品液图以及液峰对应的一级图。对图进行分析归纳,推测金霉素样品中含有四环素、差向异构四环素和差向异构金霉素杂组分。

Uranium isotope abundance ratio has been measured by total sample evaporation and signal integration,and a thermal surface ionization mass sepctrometry equipped with multicollector has been used.

采全蒸发技术、离子流强度积分的方式,多接收器热表面电离计测量铀同位素丰度。

The content of free acetic acid in cigarette smoke condensates was determined by GC-MS with isopropyl alcohol as the solvent and nonanol as the internal standard.

以异丙醇为溶剂,壬醇为内标,采气-法分析了卷烟烟气总粒物中的游离乙酸,乙酸测定结果的对标准偏差小于1%,平均回收率为99。

In this review,we described the recent development of mass spectrometry techniques for the study of peptidase structure and function in the central nerve system of Aplysia and other mollusks.

本文以海兔等软体动物为素材,综述近年来采和高效液技术研究中枢神经系统多肽酶结构与功能的进展。

The mass spectra of ureide-type noncyclic polyethers with 2(3H)-benzoxazolone as end groups were studies.

研究了以2（3H）-苯并唑酮为端基、具有酰脲结构的非环多醚的质谱。

The triphenylamine azo compounds were successfully characterized by matrix-assisted laser desorption-ionization time of flight mass spectrometry(MALDI-TOF MS).

利用基质辅助激光解吸电离飞行时间质谱法分析三苯胺偶。

Objective:To develop a GC-MS approach for the determination of tripropyltin(TPrT),tributyltin(TBT) and triphenyltin(TPhT) in fish.

建立水产品中三丙基锡、三丁基锡和三苯基锡的气相色谱-质谱(GC-MS)分析方法。

The deleterious ingredients in gas emission of sculpturing organic glass were studied,using gas chromatography-mass spectrometry coupled with 3-step preconcentrator.

研究了3阶段预浓缩气相色谱-质谱法检测有机玻璃在雕刻过程中排放的有害气体的组成。

Besides, laser optoacoustic spectroscopy technique and laser mass spectrometry will play more important role in research of internal combustion engine.

另外，激光光声光谱技术、激光质谱仪等有望在内燃机的研究中发挥更大的作用。

Dodecanol abietate succinic anhydride was synthesized from abietic acid.The structures of products were characterized by spectrum of IR，HNMR and MS.

以枞酸为起点，成了十二醇酯琥珀酸酐，采用红外光谱、核磁共振波谱及质谱对中间产及终产进行了结构表证。

In this paper ten lactonic crown ethers weresynthesized, of which seven were new compounds.Theirstructures were confirmed by EA,IR,1HNMR andMS analysis.

成了10个内酯型冠醚，中7个冠醚是新，结构均由元素分析，及红外、核磁、质谱分析证实。

The controls were homeochronous inpatients with affective disorder and normal individuals.lsoprene breath levels were measured by gas chromatography combined with mass spectroscopy(GC-MS).

用气相色谱一质谱联用仪检测呼出气体中异戊二烯的浓度。

Desorption chemical ionization mass spectrometry of twelve metallohematoporphyrin complexes has been investigated under DEP condition using mixture of tetramethylsilane and methane as regent gas.

本文以四甲基硅烷／甲烷混反应气，采用DEP技术，测定12个金属血卟啉络的解吸学电离质谱。

Based on these results and the ESI-MS data, the mechanism of sulfoxidation was proposed to be intramolecular nucleophilic oxygen transfer to a coordinated sulfide.

基于这些结果和电喷雾质谱(ESI-MS)数据，亚砜反应的机理推测为分子内亲核氧转移到络的硫醚底上。

The oils were analyzed by GC-MS and percentages were obtained by normalized peak areas, where main components are nootkatone, D-limonene, osthole, cis-linaloloxide, furfural, and trans.

用气相色谱-质谱(GC-MS)联用技术分析,鉴定出主要成分为圆柚酮、D-柠檬烯、王草素、顺式-芳樟醇氧、糠醛、反式-芳樟醇氧。

RESULTS The chlortetracycline's epimer, tetracycline and its epimer, as impurities in chlortetracycline have been determined by the liquid chromatogram and its first order mass spectrum.

结果得到金霉素样品液相色谱图以及液相色谱峰对应的一级质谱图。对谱图进行分析归纳,推测金霉素样品中含有四环素、差向异构四环素和差向异构金霉素杂质组分。

Uranium isotope abundance ratio has been measured by total sample evaporation and signal integration,and a thermal surface ionization mass sepctrometry equipped with multicollector has been used.

采用全蒸发技术、离子流强度积分的方式,用多接收器热表面电离质谱计测量铀同位素丰度。

The content of free acetic acid in cigarette smoke condensates was determined by GC-MS with isopropyl alcohol as the solvent and nonanol as the internal standard.

以异丙醇为溶剂,壬醇为内标,采用气相色谱-质谱法分析了卷烟烟气总粒相中的游离乙酸,乙酸测定结果的相对标准偏差小于1%,平均回收率为99。

In this review,we described the recent development of mass spectrometry techniques for the study of peptidase structure and function in the central nerve system of Aplysia and other mollusks.

本文以海兔等软体动为素材,综述近年来采用质谱和高效液相色谱技术研究中枢神经系统多肽酶结构与功能的进展。

The mass spectra of ureide-type noncyclic polyethers with 2(3H)-benzoxazolone as end groups were studies.

研究了以2（3H）-苯并唑酮为端基、具有酰脲结构的非环多醚化合物的质谱。

The triphenylamine azo compounds were successfully characterized by matrix-assisted laser desorption-ionization time of flight mass spectrometry(MALDI-TOF MS).

利用基质辅助激光解吸电离飞行时间质谱法分析三苯胺偶氮化合物。

Objective:To develop a GC-MS approach for the determination of tripropyltin(TPrT),tributyltin(TBT) and triphenyltin(TPhT) in fish.

建立水产品三丙基锡、三丁基锡和三苯基锡的气相色谱-质谱(GC-MS)分析方法。

The deleterious ingredients in gas emission of sculpturing organic glass were studied,using gas chromatography-mass spectrometry coupled with 3-step preconcentrator.

研究了3阶段预浓缩气相色谱-质谱法检测有机玻璃在雕刻过放的有害气体的组成。

Besides, laser optoacoustic spectroscopy technique and laser mass spectrometry will play more important role in research of internal combustion engine.

另外，激光光声光谱技术、激光质谱仪等有望在内燃机的研究发挥更大的作用。

Dodecanol abietate succinic anhydride was synthesized from abietic acid.The structures of products were characterized by spectrum of IR，HNMR and MS.

以枞酸为起点，合成了酯琥珀酸酐，采用红外光谱、核磁共振波谱及质谱对间产物及终产物进行了结构表证。

In this paper ten lactonic crown ethers weresynthesized, of which seven were new compounds.Theirstructures were confirmed by EA,IR,1HNMR andMS analysis.

合成了10个内酯型冠醚化合物，其7个冠醚是新化合物，其结构均由元素分析，及红外、核磁、质谱分析证实。

The controls were homeochronous inpatients with affective disorder and normal individuals.lsoprene breath levels were measured by gas chromatography combined with mass spectroscopy(GC-MS).

用气相色谱一质谱联用仪检测其呼出气体异戊烯的浓度。

Desorption chemical ionization mass spectrometry of twelve metallohematoporphyrin complexes has been investigated under DEP condition using mixture of tetramethylsilane and methane as regent gas.

本文以四甲基硅烷／甲烷混合反应气，采用DEP技术，测定12个金属血卟啉络合物的解吸化学电离质谱。

Based on these results and the ESI-MS data, the mechanism of sulfoxidation was proposed to be intramolecular nucleophilic oxygen transfer to a coordinated sulfide.

基于这些结果和电喷雾质谱(ESI-MS)数据，亚砜化反应的机理推测为分子内亲核氧转移到络合的硫醚底物上。

The oils were analyzed by GC-MS and percentages were obtained by normalized peak areas, where main components are nootkatone, D-limonene, osthole, cis-linaloloxide, furfural, and trans.

用气相色谱-质谱(GC-MS)联用技术分析,鉴定出主要成分为圆柚酮、D-柠檬烯、王草素、顺式-芳樟氧化物、糠醛、反式-芳樟氧化物。

RESULTS The chlortetracycline's epimer, tetracycline and its epimer, as impurities in chlortetracycline have been determined by the liquid chromatogram and its first order mass spectrum.

结果得到金霉素样品液相色谱图以及液相色谱峰对应的一级质谱图。对谱图进行分析归纳,推测金霉素样品含有四环素、差向异构四环素和差向异构金霉素杂质组分。

Uranium isotope abundance ratio has been measured by total sample evaporation and signal integration,and a thermal surface ionization mass sepctrometry equipped with multicollector has been used.

采用全蒸发技术、离子流强度积分的方式,用多接收器热表面电离质谱计测量铀同位素丰度。

The content of free acetic acid in cigarette smoke condensates was determined by GC-MS with isopropyl alcohol as the solvent and nonanol as the internal standard.

以异丙为溶剂,壬为内标,采用气相色谱-质谱法分析了卷烟烟气总粒相物的游离乙酸,乙酸测定结果的相对标准偏差小于1%,平均回收率为99。

In this review,we described the recent development of mass spectrometry techniques for the study of peptidase structure and function in the central nerve system of Aplysia and other mollusks.

本文以海兔等软体动物为素材,综述近年来采用质谱和高效液相色谱技术研究枢神经系统多肽酶结构与功能的进展。

The mass spectra of ureide-type noncyclic polyethers with 2(3H)-benzoxazolone as end groups were studies.

研究了以2（3H）-苯并唑酮为端基、具有酰脲结构的非环多醚化合物的。

The triphenylamine azo compounds were successfully characterized by matrix-assisted laser desorption-ionization time of flight mass spectrometry(MALDI-TOF MS).

用基辅助激光解吸电离飞行时间法分析三苯胺偶氮化合物。

Objective:To develop a GC-MS approach for the determination of tripropyltin(TPrT),tributyltin(TBT) and triphenyltin(TPhT) in fish.

建立水产品中三丙基锡、三丁基锡和三苯基锡的气相色-(GC-MS)分析方法。

The deleterious ingredients in gas emission of sculpturing organic glass were studied,using gas chromatography-mass spectrometry coupled with 3-step preconcentrator.

研究了3阶段预浓缩气相色-法检测有机玻璃在雕刻过程中排放的有害气体的组成。

Besides, laser optoacoustic spectroscopy technique and laser mass spectrometry will play more important role in research of internal combustion engine.

另外，激光光声光技术、激光仪等有望在内燃机的研究中发挥更大的作用。

Dodecanol abietate succinic anhydride was synthesized from abietic acid.The structures of products were characterized by spectrum of IR，HNMR and MS.

以枞酸为起点，合成了十二醇酯琥珀酸酐，采用红外光、核磁共振波及对中间产物及终产物进行了结构表证。

In this paper ten lactonic crown ethers weresynthesized, of which seven were new compounds.Theirstructures were confirmed by EA,IR,1HNMR andMS analysis.

合成了10个内酯型冠醚化合物，其中7个冠醚是新化合物，其结构均由元素分析，及红外、核磁、分析证实。

The controls were homeochronous inpatients with affective disorder and normal individuals.lsoprene breath levels were measured by gas chromatography combined with mass spectroscopy(GC-MS).

用气相色联用仪检测其呼出气体中异戊二烯的浓度。

Desorption chemical ionization mass spectrometry of twelve metallohematoporphyrin complexes has been investigated under DEP condition using mixture of tetramethylsilane and methane as regent gas.

本文以四甲基硅烷／甲烷混合反应气，采用DEP技术，测定12个金属血卟啉络合物的解吸化学电离。

Based on these results and the ESI-MS data, the mechanism of sulfoxidation was proposed to be intramolecular nucleophilic oxygen transfer to a coordinated sulfide.

基于这些结果和电喷雾(ESI-MS)数据，亚砜化反应的机理推测为分子内亲核氧转移到络合的硫醚底物上。

The oils were analyzed by GC-MS and percentages were obtained by normalized peak areas, where main components are nootkatone, D-limonene, osthole, cis-linaloloxide, furfural, and trans.

用气相色-(GC-MS)联用技术分析,鉴定出主要成分为圆柚酮、D-柠檬烯、王草素、顺式-芳樟醇氧化物、糠醛、反式-芳樟醇氧化物。

RESULTS The chlortetracycline's epimer, tetracycline and its epimer, as impurities in chlortetracycline have been determined by the liquid chromatogram and its first order mass spectrum.

结果得到金霉素样品液相色图以及液相色峰对应的级图。对图进行分析归纳,推测金霉素样品中含有四环素、差向异构四环素和差向异构金霉素杂组分。

Uranium isotope abundance ratio has been measured by total sample evaporation and signal integration,and a thermal surface ionization mass sepctrometry equipped with multicollector has been used.

采用全蒸发技术、离子流强度积分的方式,用多接收器热表面电离计测量铀同位素丰度。

The content of free acetic acid in cigarette smoke condensates was determined by GC-MS with isopropyl alcohol as the solvent and nonanol as the internal standard.

以异丙醇为溶剂,壬醇为内标,采用气相色-法分析了卷烟烟气总粒相物中的游离乙酸,乙酸测定结果的相对标准偏差小于1%,平均回收率为99。

In this review,we described the recent development of mass spectrometry techniques for the study of peptidase structure and function in the central nerve system of Aplysia and other mollusks.

本文以海兔等软体动物为素材,综述近年来采用和高效液相色技术研究中枢神经系统多肽酶结构与功能的进展。

The mass spectra of ureide-type noncyclic polyethers with 2(3H)-benzoxazolone as end groups were studies.

研究以2（3H）-苯并唑酮为端基、具有酰脲结构的非环多醚化合物的。

The triphenylamine azo compounds were successfully characterized by matrix-assisted laser desorption-ionization time of flight mass spectrometry(MALDI-TOF MS).

利用基辅助激光解吸电离飞时间法分析三苯胺偶氮化合物。

Objective:To develop a GC-MS approach for the determination of tripropyltin(TPrT),tributyltin(TBT) and triphenyltin(TPhT) in fish.

建立水产品中三丙基锡、三丁基锡和三苯基锡的气相色-(GC-MS)分析方法。

The deleterious ingredients in gas emission of sculpturing organic glass were studied,using gas chromatography-mass spectrometry coupled with 3-step preconcentrator.

研究3阶段预浓缩气相色-法检测有机玻璃在雕刻过程中排放的有害气体的组成。

Besides, laser optoacoustic spectroscopy technique and laser mass spectrometry will play more important role in research of internal combustion engine.

另外，激光光声光技术、激光仪等有望在内燃机的研究中发挥更大的作用。

Dodecanol abietate succinic anhydride was synthesized from abietic acid.The structures of products were characterized by spectrum of IR，HNMR and MS.

以枞酸为起点，合成十二醇酯琥珀酸酐，采用红外光、核磁共振波及对中间产物及终产物结构表证。

In this paper ten lactonic crown ethers weresynthesized, of which seven were new compounds.Theirstructures were confirmed by EA,IR,1HNMR andMS analysis.

合成10个内酯型冠醚化合物，其中7个冠醚是新化合物，其结构均由元素分析，及红外、核磁、分析证实。

The controls were homeochronous inpatients with affective disorder and normal individuals.lsoprene breath levels were measured by gas chromatography combined with mass spectroscopy(GC-MS).

用气相色一联用仪检测其呼出气体中异戊二烯的浓度。

Desorption chemical ionization mass spectrometry of twelve metallohematoporphyrin complexes has been investigated under DEP condition using mixture of tetramethylsilane and methane as regent gas.

本文以四甲基硅烷／甲烷混合反应气，采用DEP技术，测定12个金属血卟啉络合物的解吸化学电离。

Based on these results and the ESI-MS data, the mechanism of sulfoxidation was proposed to be intramolecular nucleophilic oxygen transfer to a coordinated sulfide.

基于这些结果和电喷雾(ESI-MS)数据，亚砜化反应的机理推测为分子内亲核氧转移到络合的硫醚底物上。

The oils were analyzed by GC-MS and percentages were obtained by normalized peak areas, where main components are nootkatone, D-limonene, osthole, cis-linaloloxide, furfural, and trans.

用气相色-(GC-MS)联用技术分析,鉴定出主要成分为圆柚酮、D-柠檬烯、王草素、顺式-芳樟醇氧化物、糠醛、反式-芳樟醇氧化物。

RESULTS The chlortetracycline's epimer, tetracycline and its epimer, as impurities in chlortetracycline have been determined by the liquid chromatogram and its first order mass spectrum.

结果得到金霉素样品液相色图以及液相色峰对应的一级图。对图分析归纳,推测金霉素样品中含有四环素、差向异构四环素和差向异构金霉素杂组分。

Uranium isotope abundance ratio has been measured by total sample evaporation and signal integration,and a thermal surface ionization mass sepctrometry equipped with multicollector has been used.

采用全蒸发技术、离子流强度积分的方式,用多接收器热表面电离计测量铀同位素丰度。

The content of free acetic acid in cigarette smoke condensates was determined by GC-MS with isopropyl alcohol as the solvent and nonanol as the internal standard.

以异丙醇为溶剂,壬醇为内标,采用气相色-法分析卷烟烟气总粒相物中的游离乙酸,乙酸测定结果的相对标准偏差小于1%,平均回收率为99。

In this review,we described the recent development of mass spectrometry techniques for the study of peptidase structure and function in the central nerve system of Aplysia and other mollusks.

本文以海兔等软体动物为素材,综述近年来采用和高效液相色技术研究中枢神经系统多肽酶结构与功能的展。

The mass spectra of ureide-type noncyclic polyethers with 2(3H)-benzoxazolone as end groups were studies.

研究了以2（3H）-苯并唑酮为端、具有酰脲结构的非环多醚化合物的谱。

The triphenylamine azo compounds were successfully characterized by matrix-assisted laser desorption-ionization time of flight mass spectrometry(MALDI-TOF MS).

利用助激光解吸电离飞行时间谱法分析三苯胺偶氮化合物。

Objective:To develop a GC-MS approach for the determination of tripropyltin(TPrT),tributyltin(TBT) and triphenyltin(TPhT) in fish.

建立水产品中三丙锡、三丁锡和三苯锡的谱-谱(GC-MS)分析方法。

The deleterious ingredients in gas emission of sculpturing organic glass were studied,using gas chromatography-mass spectrometry coupled with 3-step preconcentrator.

研究了3阶段预浓缩谱-谱法检测有机玻璃在雕刻过程中排放的有害体的组成。

Besides, laser optoacoustic spectroscopy technique and laser mass spectrometry will play more important role in research of internal combustion engine.

另外，激光光声光谱技术、激光谱仪等有望在内燃机的研究中发挥更大的作用。

Dodecanol abietate succinic anhydride was synthesized from abietic acid.The structures of products were characterized by spectrum of IR，HNMR and MS.

以枞酸为起点，合成了十二醇酯琥珀酸酐，采用红外光谱、核磁共振波谱及谱对中间产物及终产物进行了结构表证。

In this paper ten lactonic crown ethers weresynthesized, of which seven were new compounds.Theirstructures were confirmed by EA,IR,1HNMR andMS analysis.

合成了10个内酯型冠醚化合物，其中7个冠醚是新化合物，其结构均由元素分析，及红外、核磁、谱分析证实。

The controls were homeochronous inpatients with affective disorder and normal individuals.lsoprene breath levels were measured by gas chromatography combined with mass spectroscopy(GC-MS).

用谱一谱联用仪检测其呼出体中异戊二烯的浓度。

Desorption chemical ionization mass spectrometry of twelve metallohematoporphyrin complexes has been investigated under DEP condition using mixture of tetramethylsilane and methane as regent gas.

本文以四甲硅烷／甲烷混合反应，采用DEP技术，测定12个金属血卟啉络合物的解吸化学电离谱。

Based on these results and the ESI-MS data, the mechanism of sulfoxidation was proposed to be intramolecular nucleophilic oxygen transfer to a coordinated sulfide.

于这些结果和电喷雾谱(ESI-MS)数据，亚砜化反应的机理推测为分子内亲核氧转移到络合的硫醚底物上。

The oils were analyzed by GC-MS and percentages were obtained by normalized peak areas, where main components are nootkatone, D-limonene, osthole, cis-linaloloxide, furfural, and trans.

用谱-谱(GC-MS)联用技术分析,鉴定出主要成分为圆柚酮、D-柠檬烯、王草素、顺式-芳樟醇氧化物、糠醛、反式-芳樟醇氧化物。

RESULTS The chlortetracycline's epimer, tetracycline and its epimer, as impurities in chlortetracycline have been determined by the liquid chromatogram and its first order mass spectrum.

结果得到金霉素样品液谱图以及液谱峰对应的一级谱图。对谱图进行分析归纳,推测金霉素样品中含有四环素、差向异构四环素和差向异构金霉素杂组分。

Uranium isotope abundance ratio has been measured by total sample evaporation and signal integration,and a thermal surface ionization mass sepctrometry equipped with multicollector has been used.

采用全蒸发技术、离子流强度积分的方式,用多接收器热表面电离谱计测量铀同位素丰度。

The content of free acetic acid in cigarette smoke condensates was determined by GC-MS with isopropyl alcohol as the solvent and nonanol as the internal standard.

以异丙醇为溶剂,壬醇为内标,采用谱-谱法分析了卷烟烟总粒物中的游离乙酸,乙酸测定结果的对标准偏差小于1%,平均回收率为99。

In this review,we described the recent development of mass spectrometry techniques for the study of peptidase structure and function in the central nerve system of Aplysia and other mollusks.

本文以海兔等软体动物为素材,综述近年来采用谱和高效液谱技术研究中枢神经系统多肽酶结构与功能的进展。

The mass spectra of ureide-type noncyclic polyethers with 2(3H)-benzoxazolone as end groups were studies.

研究以2（3H）-并唑酮为端、具有酰脲结构的非环多醚化合物的质谱。

The triphenylamine azo compounds were successfully characterized by matrix-assisted laser desorption-ionization time of flight mass spectrometry(MALDI-TOF MS).

利用质辅助激光解吸电离飞行时间质谱法分析胺偶氮化合物。

Objective:To develop a GC-MS approach for the determination of tripropyltin(TPrT),tributyltin(TBT) and triphenyltin(TPhT) in fish.

建立水产品中丙锡、丁锡和锡的气相色谱-质谱(GC-MS)分析方法。

The deleterious ingredients in gas emission of sculpturing organic glass were studied,using gas chromatography-mass spectrometry coupled with 3-step preconcentrator.

研究3阶段预浓缩气相色谱-质谱法检测有机玻璃在雕刻过程中排放的有害气体的组。

Besides, laser optoacoustic spectroscopy technique and laser mass spectrometry will play more important role in research of internal combustion engine.

另外，激光光声光谱技术、激光质谱仪等有望在内燃机的研究中发挥更大的作用。

Dodecanol abietate succinic anhydride was synthesized from abietic acid.The structures of products were characterized by spectrum of IR，HNMR and MS.

以枞酸为起点，合十二醇酯琥珀酸酐，采用红外光谱、核磁共振波谱及质谱对中间产物及终产物进行结构表证。

In this paper ten lactonic crown ethers weresynthesized, of which seven were new compounds.Theirstructures were confirmed by EA,IR,1HNMR andMS analysis.

合10内酯型冠醚化合物，其中7冠醚是新化合物，其结构均由元素分析，及红外、核磁、质谱分析证实。

The controls were homeochronous inpatients with affective disorder and normal individuals.lsoprene breath levels were measured by gas chromatography combined with mass spectroscopy(GC-MS).

用气相色谱一质谱联用仪检测其呼出气体中异戊二烯的浓度。

Desorption chemical ionization mass spectrometry of twelve metallohematoporphyrin complexes has been investigated under DEP condition using mixture of tetramethylsilane and methane as regent gas.

本文以四甲硅烷／甲烷混合反应气，采用DEP技术，测定12金属血卟啉络合物的解吸化学电离质谱。

Based on these results and the ESI-MS data, the mechanism of sulfoxidation was proposed to be intramolecular nucleophilic oxygen transfer to a coordinated sulfide.

于这些结果和电喷雾质谱(ESI-MS)数据，亚砜化反应的机理推测为分子内亲核氧转移到络合的硫醚底物上。

The oils were analyzed by GC-MS and percentages were obtained by normalized peak areas, where main components are nootkatone, D-limonene, osthole, cis-linaloloxide, furfural, and trans.

用气相色谱-质谱(GC-MS)联用技术分析,鉴定出主要分为圆柚酮、D-柠檬烯、王草素、顺式-芳樟醇氧化物、糠醛、反式-芳樟醇氧化物。

RESULTS The chlortetracycline's epimer, tetracycline and its epimer, as impurities in chlortetracycline have been determined by the liquid chromatogram and its first order mass spectrum.

结果得到金霉素样品液相色谱图以及液相色谱峰对应的一级质谱图。对谱图进行分析归纳,推测金霉素样品中含有四环素、差向异构四环素和差向异构金霉素杂质组分。

Uranium isotope abundance ratio has been measured by total sample evaporation and signal integration,and a thermal surface ionization mass sepctrometry equipped with multicollector has been used.

采用全蒸发技术、离子流强度积分的方式,用多接收器热表面电离质谱计测量铀同位素丰度。

The content of free acetic acid in cigarette smoke condensates was determined by GC-MS with isopropyl alcohol as the solvent and nonanol as the internal standard.

以异丙醇为溶剂,壬醇为内标,采用气相色谱-质谱法分析卷烟烟气总粒相物中的游离乙酸,乙酸测定结果的相对标准偏差小于1%,平均回收率为99。

In this review,we described the recent development of mass spectrometry techniques for the study of peptidase structure and function in the central nerve system of Aplysia and other mollusks.

本文以海兔等软体动物为素材,综述近年来采用质谱和高效液相色谱技术研究中枢神经系统多肽酶结构与功能的进展。