Levocetirizine Dihydrochloride was prepared from benzoyl chloride by acidylation,hydrogenation,cyclization with an overall yield of 8.05%.
苯甲酰氯为原料,经酰化,还原,环合等反应合成左旋西替利嗪盐酸盐,反应总收率为8.05%。
Levocetirizine Dihydrochloride was prepared from benzoyl chloride by acidylation,hydrogenation,cyclization with an overall yield of 8.05%.
苯甲酰氯为原料,经酰化,还原,环合等反应合成左旋西替利嗪盐酸盐,反应总收率为8.05%。
Application of samarium diiodide in mediating intramolecular cyclization reactions was reviewed.
综述了二碘化钐在分子内环化反应中的应用。
Method The target compound was synthesized from clarithromycin via hydrolyzation,acetylation,cyclic carbonatation,oxidation,decarbonatation,acylation,cyclic carbamatation and cyclization.
方法克拉霉素为起始原料,经水解、
酰化、环
酸酯化、氧化、脱
酸酯化、酰化、环氨
甲酸酯化和环合等反应合成目标化合物。
N butyl 2 ethoxy thioacridone was prepared from o chloro benzoic acid and p phenetidine by means of Ullman reaction,cyclization,N alkylation and sulfurization.
邻氯苯甲酸和对
氧
苯胺为原料,经过胺的苯
化、二芳胺的环化、N-烷
化、硫代化反应合成了N-
-2-
氧
硫代吖啶酮。
This paper reports the improvement on the synthesis of 5 methylisoxazol 3 formamide by Claisen condensation of diethyl oxalacetate followed by cyclization and ammonolysis.
讨论了草酸二
酯为原料,经过克莱森缩合、环合、氨解反应合成5甲
异唑3甲酰胺工艺的改进。
In this paper, the synthesis of 2 - chloranthraquinone and 2 - aminoanthraquinone was studied.It was prepared from phthalic anhydride by acetyiation, hydrolysis and cyclization.
苯酐和取代苯为原料,经过
酰化、水解及环合反应,合成了2-氯蒽醌和2-氨
蒽醌,并对影响收率的工艺条件进行了研究。
Aqueous titanium trichloride promoted intermolecular reductive cyclization of 1,2 -diketone and o-nitroaniline in basic media provides a convenient method for the synthesis of quinoxaline derivatives.
本文研究了三氯化钛水溶液作用下,邻硝苯胺与1,2-二酮在碱性介质中分子间的成环反应,提供了一个方便地合成取代喹喔啉类化合物的方法。
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